RADIATION PROTECTION ›› 2016, Vol. 36 ›› Issue (4): 240-243.

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Research for the determination of radiocarbon in environmental water by bubbling and CO2 direct absorption

Yang Hailan, Bao Li, Ma Xiongnan, Gao Zequan, Meng Liping, Ren Xiaona   

  1. China Institute for Radiation Protection, Taiyuan 030006
  • Received:2015-05-22 Online:2016-07-20 Published:2021-11-15

Abstract: After the analysis and comparison of the four methods (precipitate, direct absorption, benzene synthesis and AMS) used in determining radiocarbon, bubbling and direct absorption methods were adopted to measure 14C environmental water. 50 L water was put into flask, then H3PO4 was added, and the DIC in water sample was dissolved to form CO2 by nitrogen bubbling. Released CO2 is trapped in a sodium hydroxide molar solution before being precipitated as calcium carbonate. Calcium carbonate from water is acidified to release CO2. CO2 is absorbed by Carb-sorb E measured by LSC. The recovery was proven to be 90.3% and the limit detection is 0.2 mBq/L.This method was used to analyze different water samples of Fujian province results of radiocarbon activity concentrations of which are between 1.31—10.26 mBq/L.

Key words: radiocarbon, environmental water, inorganic carbon, direct absorption method

CLC Number: 

  • O657